在线氰化物监测仪

在线氰化物监测仪

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CYANIDE

Cyanide is used in industrial applications ranging from organic synthesis in a chemical plant to precious metal plating. Due to high toxicity, HCN is also a priority pollutant which must be measured on-line to meet federal and state permitted release levels.

A typical application in an HCN production plant would be the measurement of cyanide in effluent waters before chlorination in a cyanide destruction process, and another application would be monitoring low levels of cyanide in waste recovery just prior to final effluent release. In both applications the objectives are:

  • to document that such releases are within permit and
  • to provide feedback control to prevent releases above permitted levels.

TYTRONICS'® SENTINEL

Tytronics’ Sentinel is an on-line colorimetric analyzer. The instrument uses a batch sampling technique that allows the use of 0.25" tubing for sample lines, so small amounts of solids will not affect instrument performance. Other advantages of batch sampling are:

  • analytical results are not affected by sample and reagent flows;
  • analyses are only performed as frequently as required, minimizing reagent consumption.

METHOD

This colorimetric analysis uses 2 ml each of reagent 1, reagent 2 and reagent 3. 

Method:

Colorimetric

Measurement range:

0-100 ppb

Sample size:

30 ml

Reagent 1:

phosphate buffer/ chloramine T

Reagent 2:

4-picoline, sodium hydroxide/EDTA

Reagent 3:

potassium carbonate/ methanol/3-methyl-1-phenyl-2-pyrazoline-5-one

Volume/analysis each reagent

2 ml

Measurement Wavelength

630 nm

Reference Wavelength

810 nm

Analysis Time

15minutes

Enhanced Features of Tytronics’ Sentinel:

  • Programmable from 1 to 10 methods for a single analysis compound;
  • Up to 3 different calibration methods;
  • Eight relay outputs, multi-programmable on each relay;
  • Alarm functions, including sample flow, reagent level detection;
  • From 1 to 6 stream configurations standard.

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